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Thread: permeate .7 ?

  1. #1
    Join Date
    Sep 2015
    Location
    Rumney NH
    Posts
    126

    Default permeate .7 ?

    hello Traders,maybe you can help me though this. ran my ro today for the first time. on sap. set pressure at300 with recirculating needle valve open . permeate meter was running at 3.5 and concentrate meter at .5. almost right at original owners marks on flow meters. permeate was a little higher. sap sugar was 1.3% going in 5% coming out concentrate side, .7% coming out permeate side? is this normal? it's a waterloo- small 300gph antique. I shut the ro down when I realized it. maybe 100 gallons of sap. it does have a lot of leaks, one's pretty big at 300 psi. feel like i'm missing something. any pointers would be much appreciated.
    2017 140 taps 30x8 12x16 shack 28.5 gal
    2018 158 taps 30x8 12x16 shack with 8x8 kitchen 44 gal
    2019 223 taps 30x8 12x16 shack with 8x8 kitchen 36 gal
    2020 226 taps 30x8 12x16 shack with 8x8 kitchen 250 waterloo ro 63 gal
    2021 230 taps 30x8 12x16 shack with 8x8 kitchen 250 waterloo ro 37 gal
    2022 230 taps 30x8 12x16 shack with 8x8 kitchen 250 waterloo ro 55 gal
    2023 235 taps 30x8 12x16 waterloo ro 50 gal
    2024 54gal

  2. #2
    Join Date
    Jan 2010
    Location
    Covington, New York
    Posts
    1,680

    Default

    Seems like you are passing sugar. Mine reads negative .5 which leads me to believe my hydrometer is off a little
    Noel Good
    1998 to 2009: 15 taps on buckets, scavenged fire pit and pans
    2010: New 2x4 SS flat pan w/preheater
    2015: New to me Lapierre 18x60 raised flue, new shack, new everything!! 59 taps 23.75 gallons
    2016: 85 taps 19 gallons
    2017: Purchased 2.5 acres and tubed half with 3/16. 145 taps total 49.25 gallons
    2018: 200 taps (162 on 3/16ths 38 on buckets) New NextGen RO 63 gallons
    2019: 210 taps 73.5 gallons
    2023: 210 taps 89.75 gallons
    www.wnybass.com

  3. #3
    Join Date
    Aug 2017
    Location
    Wadsworth, OH
    Posts
    120

    Default

    300 psi seems high to me to be running at but I'm not familiar with that machine and it's specs. My machine says not to exceed 225 psi, and I rarely go above 150...
    Mike

    450 taps on vacuum - 2018 - 150 gal
    530 taps on vacuum - 2019 - 190 gal
    520 taps on vacuum - 2020 - 196 gal
    515 taps on vacuum - 2021 - 150 gal
    24 x 32 Pole Barn Sugar House 2018
    Smoky Lake 2x8 Silverlake Raised Flue w/ concentric exhaust 2018
    Memprotec 350H RO
    Smoky Lake Water Jacket Bottler 2018
    Smoky Lake Filter Press 2018
    Smoky Lake Water Jacket Draw Off Tank 2018

  4. #4
    Join Date
    Sep 2015
    Location
    Rumney NH
    Posts
    126

    Default

    wnybassman,
    it does seem like I'm passing sugar. but where? bad membrane, o-ring , membrane not seated right, plug and two little O-rings on it in the end of membrane are the only things that could cause this .correct.

    miboss,
    says on front panel not to exceed 500psi . my flow meters don't level out until 200psi unless i'm doing something wrong. I did say- ran my ro today for the first time. on sap.
    2017 140 taps 30x8 12x16 shack 28.5 gal
    2018 158 taps 30x8 12x16 shack with 8x8 kitchen 44 gal
    2019 223 taps 30x8 12x16 shack with 8x8 kitchen 36 gal
    2020 226 taps 30x8 12x16 shack with 8x8 kitchen 250 waterloo ro 63 gal
    2021 230 taps 30x8 12x16 shack with 8x8 kitchen 250 waterloo ro 37 gal
    2022 230 taps 30x8 12x16 shack with 8x8 kitchen 250 waterloo ro 55 gal
    2023 235 taps 30x8 12x16 waterloo ro 50 gal
    2024 54gal

  5. #5
    Join Date
    Jan 2010
    Location
    Covington, New York
    Posts
    1,680

    Default

    You did say it had a lot of leaks, I am assuming on the outside. Perhaps there are leaks on the inside as well.
    Noel Good
    1998 to 2009: 15 taps on buckets, scavenged fire pit and pans
    2010: New 2x4 SS flat pan w/preheater
    2015: New to me Lapierre 18x60 raised flue, new shack, new everything!! 59 taps 23.75 gallons
    2016: 85 taps 19 gallons
    2017: Purchased 2.5 acres and tubed half with 3/16. 145 taps total 49.25 gallons
    2018: 200 taps (162 on 3/16ths 38 on buckets) New NextGen RO 63 gallons
    2019: 210 taps 73.5 gallons
    2023: 210 taps 89.75 gallons
    www.wnybass.com

  6. #6
    Join Date
    Feb 2013
    Location
    Marysville, Ohio
    Posts
    663

    Default

    It does sound like the membrane is passing some sugar if your flow meter readings are correct. You should be seeing 8-9% concentrate instead of 5%. It is very difficult to measure sugar content accurately down between 0-1% but 0.7 is pretty high relative to 1.3% sap. You could have 3 possibilities. 1) The membrane could be passing sugar because of it's age and being cleaned under too high a pH or too high temperature or the pressure it just too high at 300 psi. 2) the membrane could be physically damaged by over pressure on the permeate side at one time in the past or 3) the small o-rings on the inside are damaged and need to be replaced. I guess there could be other possibilities but these are the most likely. I would try running the pressure at 225 to 250 psi. A nano-filtration membrane such as an NF 270 that has been cleaned several times may pass quite a bit of sugar at 300 psi. If that doesn't help you can replace the small internal o-rings. If it's still passing sugar at the lower pressure and the o-rings are new then it's most likely a damaged membrane and the only thing you can do is replace the membrane or live with the problem.
    Leader 1/2 pint - Kawasaki Mule - Smoky Lake Filter Bottler
    24 GPH RO, 2 1/2 x 40 NF3 (NF270), 140 GPH (Brass with no relief valve ) ProCon pump
    2013 - 44 taps - 16 gallons syrup, 2014 - 109 taps - 26 gallons syrup
    2015 - 71 taps - 13.5 gallons syrup, 2016 - 125 taps - 24.25 gallons syrup
    2017 - 129 taps - 17.5 gallons syrup, 2018 - 128 taps- 18 gallons syrup
    2019 -130 taps - 18.5 gallons syrup, 2020 ~125 taps-19.75 gallons syrup

  7. #7
    Join Date
    Jan 2006
    Location
    Oneida NY
    Posts
    11,564

    Default

    If the RO was running correctly and the membrane(s) are in good condition the permeate should be at or very near 0.0 sugar. I suspect the membrane(s) need replacing but it could be another issue. Could be a bad seal too, allowing some concentrate to leak into the permeate side, but the membrane(s) are most likely the issue.
    Dave Klish, I recently ordered a 2x6 wood fired evaporator from A&A Sheet Metal which I will be converting to oil fired
    Now have solar, 2x6 finish pan, 5 bank 7x7 filter press, large water jacketed bottler, and tankless water heater.
    Recently bought another Gingerich RO, this one was a 125, but a second membrane was added thus is a 250, like I had.
    After running a 2x3, a 2x6, 3x8 tapping from 79 taps up to 1320 all woodfired, now I'm going to a 2x6 oil fired and a 200-425 taps.

  8. #8
    Join Date
    Dec 2002
    Location
    Rock Creek, NC
    Posts
    5,807

    Default

    It sounds like you're passing sugar. Most membranes can handle 600 psi and a lot of the older professional RO's can run at up to 500 psi. Mine has a high pressure switch that shuts it off at 500 psi. What membrane do you have? If it's a Dow NF-270 it can pass sugar at higher pressures and concentration levels. Did it get damaged by drying out or freezing? Is the U-cup installed properly, if it uses one? Is the big O-ring seal on the membrane facing the right direction? If you find that you need to replace your membrane, or membranes, if you have more than one give MES a call. I bought two of their MS2 4" membranes for $215 each. They flow fast and don't pass sugar. I've been running mine at 300 to 400 psi and I don't think running your's at 300 psi is the cause of your problem.
    Russ

    "Red Roof Maples" Where the term "boiling soda" was first introduced to the maple world!

    1930 Ford Model AA Doodlebug tractor
    A couple of Honda 4 wheelers
    Four chainsaws and no chickens!

  9. #9
    Join Date
    Sep 2015
    Location
    Rumney NH
    Posts
    126

    Default

    well the two membranes in there are osmonics desal model-dk4040f1023. says vista California on them. I could not find them on the web. just like my ro. too old. I do remember the big o-ring on the outside was in good shape. apon opening last fall I did replace 2 of the 4 little O-rings as I could see pieces of them on top of the membrane.


    Russell , Is the U-cup installed properly? I don't remember seeing one where are is it located? did you need to by the plug separate or does it come with membrane?

    thought about it all night and if I have to tare this thing down I just as well put new back in. it's just as much work. as I tare down I will keep an eye out. thanks for the replies.
    2017 140 taps 30x8 12x16 shack 28.5 gal
    2018 158 taps 30x8 12x16 shack with 8x8 kitchen 44 gal
    2019 223 taps 30x8 12x16 shack with 8x8 kitchen 36 gal
    2020 226 taps 30x8 12x16 shack with 8x8 kitchen 250 waterloo ro 63 gal
    2021 230 taps 30x8 12x16 shack with 8x8 kitchen 250 waterloo ro 37 gal
    2022 230 taps 30x8 12x16 shack with 8x8 kitchen 250 waterloo ro 55 gal
    2023 235 taps 30x8 12x16 waterloo ro 50 gal
    2024 54gal

  10. #10
    Join Date
    Dec 2002
    Location
    Rock Creek, NC
    Posts
    5,807

    Default

    Quote Originally Posted by amasonry View Post
    well the two membranes in there are osmonics desal model-dk4040f1023. says vista California on them. I could not find them on the web. just like my ro. too old. I do remember the big o-ring on the outside was in good shape. apon opening last fall I did replace 2 of the 4 little O-rings as I could see pieces of them on top of the membrane.


    Russell , Is the U-cup installed properly? I don't remember seeing one where are is it located? did you need to by the plug separate or does it come with membrane?

    thought about it all night and if I have to tare this thing down I just as well put new back in. it's just as much work. as I tare down I will keep an eye out. thanks for the replies.
    On my RO the U-cup slides over the big seal on the membrane. Because of the design of the pressure vessels some don't use them and the membrane seals against the pressure vessel directly. The plug that goes on the end of the membrane is sold separately. I suggest getting the cap style plug, not the one that goes inside the nipple. MES doesn't have the Cap style plug, get those from Lapierre. They're about $25 each but they work on any membrane with a 1/2" nipple. I'm assuming that you have 4" membranes.
    Russ

    "Red Roof Maples" Where the term "boiling soda" was first introduced to the maple world!

    1930 Ford Model AA Doodlebug tractor
    A couple of Honda 4 wheelers
    Four chainsaws and no chickens!

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